in-situ
Small/Wide-Angle X-ray scattering (SAXS/WAXS) in-situ for nanostructure and crystallinity
morphological characterization of ionomer membranes using transmission small- and wide-angle X-ray scattering (SAXS/WAXS) in situ, with capabilities to probe nanostructural and crystalline features in dry and hydrated conditions as a function of temperature (30-100% RH in ambient. from 25°C to 90°C in liquid, and up to 200°C for dry environment)
Spectrocopic Ellipsometry for Thin Film Expansion and Swelling with RH
Determine swelling of nanometer-thick ionomer thin films (10-200 nm) on supports to mimic the hydration response of electrode/catalyst ionomers in controlled environment
Microelectrode system: electro-osmotic coefficient, gas permeability and solubility testing, kinetics
Microelectrode and microcavity electrode setup to evaluate catalyst and membrane materials. Independent control of atmosphere (gas type and RH) at the working and reference electrodes